Preparation of Nickel (Ni) doped SrTiO3 and effects of sintering temperatures on its properties as photocatalyst

Firda Reza Agustina, Bachtiar Suherman, L U Hasanah, N F S Puspita,Dianisa Khoirum Sandi,Fahru Nurosyid,Erfan Handoko, Yofentina Iriani

Journal of physics(2023)

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摘要
SrTi 0.97 Ni 0.03 O 3 photocatalysts with varied sintering temperatures of 900°C and 1000°C have been successfully prepared via the co-precipitation method. This study aimed to determine the effect of temperature on SrTi 0.97 Ni 0.03 O 3 photocatalyst including the microstructure, atomic bonding, and photocatalyst activity. X-Ray Diffraction (XRD) data revealed an increase in the crystallite size with increasing the sintering temperature. Fourier Transform Infrared (FTIR) results confirmed the formation of Sr-Ti-O bonds followed by the presence of CH impurities that the impurities decreased at 1000°C. The photocatalyst activity was tested using methylene blue (MB) degradation in SrTi 0.97 Ni 0.03 O 3 photocatalysts under UV rays. The time for the irradiation process varied from 3, 4, to 5 hours. The degraded result was examined using a UV-Vis spectrophotometer to estimate the %degradation. The results demonstrated that the sintering temperatures do not considerably impact MB degradation. Further, the best treatment for SrTi 0.97 Ni 0.03 O 3 to attain the highest MB degradation of 49.9% is at 900°C with 5 hours of irradiation.
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关键词
photocatalyst,nickel,srtio<sub>3</sub>,nickel
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