1-Phosphanorbornane aldehyde as precursor for enantiopure P,N,N ligands

Kyzgaldak Ramazanova, Nadja Kretzschmar, Peter Loennecke, Evamarie Hey-Hawkins

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS（2024）

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摘要

Sulfur-protected enantiomerically pure 1-phosphanorbornane aldehyde 5 is obtained in good yield via Swern oxidation of the previously reported 1-phosphanorbornane alcohol. The aldehyde is further used to prepare a novel sulfur-protected 1-phosphanorbornane enamine. GRAPHICAL ABSTRACT

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关键词

Chirality,enamine,P-heterocycles,pincer ligands,reductive amination

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