Metal-Free Cascade O-H Double Insertion Between I(III)/S(VI)-Ylides, Carboxylic Acids, and Alcohols: Modular Access to Unsymmetrical α,α-O,O-Substituted Ketones

Shang-Shi Zhang, Jiaohang Wei, Wen-Xuan Zou,Qiong Hu, Mei-Zhu Bao,Dan-Ting Shen, Lin Xiao,Jia-Lin Song,Xiang Liu

Organic Chemistry Frontiers（2024）

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摘要

The synthesis of unsymmetrical α,α-O,O-substituted ketones via O-H double insertion is appealing but remains constrained due to the lack of compatible coupling partners or uncontrollable selectivity. Herein, we present a...

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