2-{1-[(6R,S)-3,5,5,6,8,8-Hexamethyl-5,6,7,8-tetrahydronaphthalen-2-yl]ethylidene}-N-methylhydrazinecarbothioamide

Ana Paula Lopes de Melo, Alex Fabiani Claro Flores,Leandro Bresolin,Bárbara Tirloni,Adriano Bof de Oliveira, M. Bolte

IUCrData（2023）

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摘要

The synthesis, crystal structure and Hirshfeld analysis of (R,S)-fixolide 4-methylthiosemicarbazone is reported. The compound is disordered over the fixolide fragment and in the crystal, the molecules are linked by H⋯S interactions with graph-set motif C(4), forming mono-periodic hydrogen-bonded ribbons along [100].

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关键词

thiosemicarbazone,fixolide thiosemicarbazone,chiral thiosemicarbazone,hydrogen-bonded ribbon,fixolide derivative,crystal structure

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2-{1-[(6R,S)-3,5,5,6,8,8-Hexamethyl-5,6,7,8-tetra­hydro­naphthalen-2-yl]ethyl­idene}-N-methyl­hydrazinecarbo­thioamide

2-{1-[(6R,S)-3,5,5,6,8,8-Hexamethyl-5,6,7,8-tetrahydronaphthalen-2-yl]ethylidene}-N-methylhydrazinecarbothioamide