EBSD analysis of grain boundary evolution and dynamic recrystallization of Inconel 625 superalloy at various hot spinning feed rates

Zhanjie Jing,Jiangkun Fan, Xudong Liu,Yuelin Song, Zixiao Wang,Kai Cao,Yuetan Chen, Heng Fu, Jianing Zhang,Jinshan Li

Progress in Natural Science: Materials International(2024)

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摘要
Hot spinning can make the material withstand shear stress, so that the shape of the material has a great change, which is one of the main processing methods of nickel-based alloy plate members. Inconel 625 alloy, which has excellent high temperature mechanical properties and can be used as the main candidate material for aerospace applications, needs further study on its hot spinning deformation behavior and deformation mechanism. In this paper, the effect of feed rate on the microstructure evolution of Inconel 625 superalloy was studied by the electron backscattered diffraction technology. The microstructure with necklace-like structures composed of dynamic recrystallization (DRX) grains was observed after hot spinning. It was found that at the low feed rate, the promotion of DRX degree and grain refinement happened, where the grain size reached the trough of 10.99 ​μm under a feed rate of 300 ​mm/min. However, with the further feed rate rising, the degree of DRX was suppressed to a certain extent and grain size increased to 14.26 ​μm. On balance, the feed rate of 300 ​mm/min was the most efficient condition for grain refinement. Besides, it was revealed that both discontinuous dynamic recrystallization (DDRX) and continuous dynamic recrystallization (CDRX) occurred during hot spinning. DDRX includes the initial grain boundary nucleation by bulging and the annealing twin boundary assisted nucleation, while the CDRX mechanism is related to the continuous subgrain rotation within the deformed grain. DDRX is the main DRX mechanism.
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关键词
Inconel 625 superalloy,Hot spinning,Grain boundary evolution,DRX mechanism
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