KIO3-catalyzed selective oxidation of thiols to disulfides in water under ambient conditions
ORGANIC & BIOMOLECULAR CHEMISTRY(2024)
摘要
Herein, we report a KIO3-catalyzed oxidative coupling of thiols to their corresponding disulfides in water, in a short time and at ambient temperature. The reaction has a broad scope and exhibits good functional group tolerance, resulting in the desired products in excellent yields. This approach allows the reuse of the reaction system in multiple cycles and scale-up. Furthermore, the current protocol demonstrates compatibility for in situ generation of disulfides and post application in C(sp(2))-H bond sulfenylation.
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