A Cost-Effective Way to Produce Gram-Scale 18O‑Labeled Aromatic Aldehydes

Yuan Yang,Bingyang Han,Fenghao Dong,Jiawei Lv,Huiming Lu,Yuqing Sun,Ziqiang Lei,Zengming Yang,Hengchang Ma

Organic Letters（2022）

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摘要

Obtaining 18O-labeled organic substances is of great research importance and also an extremely challenging work. In this work, depending on the reversed Knoevenagel reaction, 18O-labeled aromatic aldehydes (3a–3x) are successfully obtained with high total yields (52–72%) and sufficient 18O abundance (90.90–96.09%).

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