Sustainable and practical semi-heterogeneous photosynthesis of 5-amino-1,2,4-thiadiazoles over WS2/TEMPO
Chinese Chemical Letters(2024)
摘要
An eco-friendly and practical method for the clean preparation of 5-amino-1,2,4-thiadiazoles was developed. With WS2 as the semiconductor photocatalyst, both TEMPO and O2 (in air) as the redox catalysts, a variety of thiadiazoles were semi-heterogeneously formed in high to quantitative yields and could be easily collected by CPME extraction and rinsing. Furthermore, the catalytic system can be reusable for at least 5 reaction runs.
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关键词
Green chemistry,Thiadiazoles,Heterogeneous catalyst,Redox catalyst,Extraction
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