Copper-Catalyzed Diazidation of Allenes: Access to 3-(Azidomethyl)-2H-Azirines

Shen-Yuan Zhang, Li-Yan Hu,Yang Li,Yuan Li,Kai Luo,Lei Wu

ADVANCED SYNTHESIS & CATALYSIS（2024）

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摘要

A class of 3-(azidomethyl)-2H-azirine has been obtained through a copper-catalyzed diazidation of allenes and a subsequent azirination involving vinyl azides. A variety of functional groups in the allenes are well tolerated, providing a series of 3-(azidomethyl)-2H-azirine motifs in 51%-93% yields (26 examples).

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关键词

3-(azidomethyl)-2H-azirines,copper-catalysis,diazidation of allenes,azirination,vinyl azides

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