Two-dimensional Ti3C2 MXene-derived Ti3C2-Ti2C-TiO2 materials for improved diclofenac sodium adsorption performance
ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH(2023)
摘要
This paper aims to prepare an adsorbent based on MXene material for adsorbing diclofenac sodium (DCF). In this paper, Ti3C2-MXene was prepared by etching Ti3AlC2 with hydrofluoric acid (HF). Ti3C2 was subjected to a convenient and simple solvothermal treatment. TiO2 and Ti2C were formed during the solvothermal process. According to the results of FT-IR and XRD, the formation of TiO2 and Ti2C will increase the interlayer spacing of the prepared Ti3C2-12 h, thereby improving the adsorption performance of MXenes. The main factors affecting the adsorbent, the maximum adsorption capacity, and the interaction between the two factors were analyzed by single-factor experiment, orthogonal experiment, and response surface analysis. The maximum DCF adsorption capacities of Ti3C2 and Ti3C2-12 h are 201 mg/g and 395 mg/g, respectively. MXene made from HF can absorb DCF under various pH conditions and maintain a high adsorption rate, which has important applications in environmental protection.
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关键词
Ti3C2,Adsorption,Diclofenac sodium,Orthogonal experiments
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