Effect of Salt Roasting Factors on Water Leaching of Vanadium Concentrate by Design of Experiment

Resources Recycling(2023)

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摘要
We investigated the effect of salt roasting conditions on vanadium concentrate's water leaching by Design of Experiment (DOE). The experiments were done by a random sequence using the design of 2-level and three repetitions with a central point. The factors and their levels were roasting temperature 1000, 1200 °C, sodium sulfate ratio in sodium salt 30, 70 %. The change in factor level did not give a statistically meaningful effect on the vanadium leaching ratio based on T-test and ANOVA with a significance level of 0.05, and the vanadium leaching ratio was between 80 and 90 % in 30 minutes. In contrast, the factors and interaction had a statistically significant effect on the aluminum leaching ratio. Higher temperature and sodium sulfate ratio produce a higher aluminum leaching ratio, whereas the interaction of factors showed the opposite. Water leaching of roasted vanadium concentrate at 1000 °C/sodium sulfate ratio of 30 % and 1200 °C/70 % resulted in 8.96 % and 0 % of aluminum leaching ratio, respectively. A regression analysis produced an aluminum leaching model equation with an R-squared of 0.9960.
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vanadium concentrate,salt roasting factors,water leaching
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