Rh(III)-catalyzed selective mono- and dual-functionalization/cyclization of 1-aryl-5-aminopyrazoles with iodonium ylides

Longkun Chen,Mingshuai Zhang, Meichen Liu,Zhuoyuan Liu, Yuetong Qiu,Zhilai Zhang,Fuchao Yu,Jiuzhong Huang

Chemical Communications（2024）

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摘要

An efficient Rh(III)-catalyzed selective mono- and dual-C-H bond functionalization/cyclization with iodonium ylide as a single coupling partner was demonstrated, in which fused benzodiazepine skeletons were obtained in excellent yields. This method greatly improved an effective approach to dual C-H unsymmetrical functionalization.

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