Synthesis of a titanium ethylene complex via C–H-activation and alternative access to Cp₂Ti(η²-Me₃SiC₂SiMe₃)

Malte Fischer, Lisa Vincent-Heldt, Malena Hillje,Marc Schmidtmann,Ruediger Beckhaus

Dalton Transactions（2020）

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摘要

The synthesis of a room temperature stable titanacyclopropane in a one-step-two-transformation protocol is presented. Additionally, a novel one-pot procedure toward Cp2Ti(η2-Me3SiC2SiMe3) was subsequently developed.

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Synthesis of a titanium ethylene complex via C–H-activation and alternative access to Cp2Ti(η2-Me3SiC2SiMe3)

Synthesis of a titanium ethylene complex via C–H-activation and alternative access to Cp₂Ti(η²-Me₃SiC₂SiMe₃)