Effect of solution treatment of AZ91 alloy on microstructure, mechanical properties and corrosion behavior of friction stir back extruded AZ91/bioactive glass composite
Journal of Materials Research and Technology(2023)
摘要
In the present study, we investigated the effects of solution treatment and friction stir back extrusion on the microstructure, mechanical properties, and in-vitro corrosion behavior of the AZ91/64SiO2–31CaO–5P2O5 composite. The findings demonstrate that the reinforcing phase of bioactive glass in the AZ91 matrix exhibits a gradient distribution, resulting in grain refinement in the zone near the surface of the composite wire. The fabrication of the AZ91-3 vol% bioactive glass composite through friction stir back extrusion, utilizing a rotational speed of 1200 rpm and an extrusion speed of 20 mm/min, leads to a significant improvement in corrosion resistance compared to the solid solutionized AZ91 alloy, as demonstrated by a ∼93% increase in simulated body fluid (SBF). During the friction stir back extrusion of the solid solutionized AZ91 alloy, heat and plastic deformation result in the re-precipitation of the ß-Mg17Al12 phase in the α-Mg matrix. The presence of bioactive glass particles facilitates this re-precipitation process during friction stir back extrusion. In comparison to the solid solutionized AZ91 alloy, the AZ91-3 vol% bioactive glass composite exhibits a 23% increase in ultimate tensile strength (UTS), a 28% increase in yield strength (YS), and a 30% decrease in elongation.
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关键词
Friction stir back extrusion,Solution treatment,Bioactive glass particles,Mechanical properties,Corrosion behavior
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