Habit planes of climbing and gliding dislocations in TiAl determined in three dimensions by electron tomography

SCRIPTA MATERIALIA(2023)

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摘要
In this study, the habit planes of dislocations moving by glide and climb at 850–900 °C have been determined in three dimensions (3D) by electron tomography, using the TiAl intermetallics as a model system. An almost complete digital 3D reconstruction approach has been implemented, based on algorithms developed in life sciences, with which the habit planes orientations have been obtained with ±5° accuracy. It could thus be demonstrated, notably, that climbing a[001] pure edge dislocations loops, previously identified in literature, actually constitute Bardeen-Herring sources. Moreover, mixed-climb in {011) planes has been properly evidenced, as well as coexistence of gliding and climbing dislocation segments in the same region of the crystal. Consequently, improving the material's strength at 850–900 °C would require controlling both the glide and climb mechanisms by means of suitable solutes.
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关键词
Dislocations,Electron tomography,3D reconstruction
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