Formal synthesis of isoquinocyclinone using ortho-alkoxycarbonylmethylation of anthranol via diazoquinone

Mitsuru Kitamura, Noriyuki Fukuzumi, Masayuki Shinagawa, Keiichiro Araki, Yutaro Shimizu,Shuhei Takahashi, Takumi Iwata,Hirokazu Shimooka,Tatsuo Okauchi

Tetrahedron Letters（2023）

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摘要

•Formal synthesis of isoquinocyclinone is described.•Key transformation is ortho-alkoxycarbonylmethylation of poly-substituted anthranol via diazoquinone.•Key intermediate lactone was constructed from 1,2-dihydrotetracene-1-carboxylic acid derivative via epoxidation.

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关键词

isoquinocyclinone,anthranol,synthesis,ortho-alkoxycarbonylmethylation

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