Selective room-temperature dimethylformamide vapor sensing using MoSe2-rGO composite synthesized via facile hydrothermal method
Materials Today Communications(2023)
摘要
Two dimensional semiconductors such as MoSe2 with large specific surface area, bandgap in visible region and high carrier mobilities have attracted a greater attention as a sensing platform. A composite of MoSe2 and reduced graphene oxide (rGO) has been successfully synthesized using a facile hydrothermal method and used as a gas sensing platform for the room-temperature detection of dimethylformamide (DMF). Structural analysis has revealed the formation of MoSe2/rGO composite along with the presence of MoO3 due to partial oxidation of MoSe2 into MoO3. In addition, the presence of J2 mode (150.6 cm−1) in Raman spectra and 3d doublet with lower spin-orbit splitting in XPS spectra indicated the presence of 1T-MoSe2 in addition to main 2H-MoSe2. Sensor displayed a sensitive and selective detection of DMF down to 2 ppm with response (recovery) time of 130 s (50 s) and a relative response of 3.6 %. Present work highlights the role of optimum weight ratio in determining the overall sensing performance of the sensing devices. The advantages of repeatability, selectivity and excellent stability, provide a great possibility for the use of MoSe2/rGO-based composites in sensing.
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关键词
room-temperature
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