Synthesis of [1,2,3]‐Triazolo[1,5‐a][1,4]benzodiazepines via an Unprecedented One‐Pot Cu‐Catalyzed Azidation—Cyclization Reaction.

Geert Hooyberghs,Hendrik De Coster,Dipak D. Vachhani,Denis S. Ermolat'ev,Erik V. Van der Eycken

ChemInform（2013）

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摘要

A novel three-step approach leading to [1,2,3]-triazolo[1,5-a][1,4]benzodiazepines in moderate to good yields has been developed. The key step is an unprecedented one-pot Cu-catalyzed azidation–cyclization reaction of ortho-bromobenzylpropargylamines.

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