Sequential KO^tBu/FeCl₃-catalyzed reductive phosphonylation of tertiary amides for the synthesis of α-amino phosphonates and phosphines

Yue Wang,Xiaoyu Wu,Liqun Yang,Wei Liu,Zhaoguo Zhang,Xiaomin Xie

Organic & Biomolecular Chemistry（2023）

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摘要

A simple, mild and effective protocol involving sequential KOtBu-catalyzed hydrosilylation of tertiary amides with TMDS and FeCl3-catalyzed phosphonylation has been developed for the synthesis of α-amino phosphonates and their derivatives.

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Sequential KOtBu/FeCl3-catalyzed reductive phosphonylation of tertiary amides for the synthesis of α-amino phosphonates and phosphines

Sequential KO^tBu/FeCl₃-catalyzed reductive phosphonylation of tertiary amides for the synthesis of α-amino phosphonates and phosphines