Dimeric and 1D polymeric low-chlorinated C₆₀ fullerenes, (C₆₀Cl₅)₂ and (C₆₀Cl₄)

Victor A. A. Brotsman,Nadezhda B. B. Tamm,Ilya N. N. Ioffe,Andrei A. A. Eliseev,Alexey A. A. Goryunkov,Konstantin A. A. Lyssenko,Sergey I. I. Troyanov

DALTON TRANSACTIONS（2023）

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摘要

Low-chlorinated fullerenes, dimeric (C60Cl5)(2) and one-dimensional, polymeric (C60Cl4)(infinity), were obtained by high-temperature (270 degrees C) chlorination of C-60 with a SbCl5/SbCl3 mixture, as revealed by X-ray crystallography. The compounds were characterized by IR and Raman spectroscopy and theoretical calculations. This is the first observation of a fullerene polymer with single C-C bonding and neutral building blocks.

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Dimeric and 1D polymeric low-chlorinated C60 fullerenes, (C60Cl5)2 and (C60Cl4)

Dimeric and 1D polymeric low-chlorinated C₆₀ fullerenes, (C₆₀Cl₅)₂ and (C₆₀Cl₄)