Assembly of Benzo[ c ][1,2]dithiol-3-ones via Acid-Promoted Denitrogenative Transannulation of Benzotriazinones.
Organic letters(2022)
摘要
An expedient synthesis of benzo[][1,2]dithiol-3-ones via metal-free denitrogenative transannulation of benzotriazinones is developed, which represents the first example of acid-mediated heteroannulation of benzotriazinones. This newly discovered reactivity of benzotriazinones enables the streamline synthesis of diverse benzo[][1,2]dithiol-3-ones in decent yields by using sodium sulfide as the sulfur source under simple reaction conditions.
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关键词
benzotriazinones,acid-promoted
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