Pneumatic angle adjustment for magic angle spinning spherical rotors

Journal of Magnetic Resonance Open(2021)

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摘要
•A new stator for spinning spherical MAS rotors is designed and 3D-printed for use in an NMR probe.•The new stator enables fine and stable control of the spinning angle of a sphere rotor with no mechanical adjustment required.•The angle adjustment sensitivity is measured by observing the off-magic angle lineshape of a deuterated solid and comparing to simulated spectra.
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关键词
Angle adjustment,Spherical rotors,MAS,Pneumatic,NMR hardware,Solid state NMR
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