The radical reaction of ethynylbenziodoxolone (EBX) reagents with pentafluorosulfanyl chloride: New approach to SF5-substituted alkynes

Journal of Fluorine Chemistry（2022）

引用 4|浏览10

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摘要

•New access to SF5-substituted alkynes is developed.•Radical alkynylation is the key step of the synthesis.•Ethynylbenziodoxolones are used as alkynylating reagents.•For the first time, no base is involved in the synthesis of SF5-alkyne derivatives.

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关键词

Pentafluorosulfanylation,Alkynes,Radical reaction,Ethynylbenziodoxolone (EBX) reagent

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