Unexpected sensitivity enhancement in analysing alfatoxin M1 using LC-IDMS

Adam Tolgyesi, Bence Toth Kovacs,Edgar Toth,Andrea Simon,Maria Balint,Virender K. Sharma

Microchemical Journal（2022）

引用 3|浏览3

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摘要

•New LC-MS/MS determination is demonstrated for analyzing aflatoxin M1.•Neutral mobile phase composition gives enhanced selectivity and sensitivity.•The separation is carried out on mixed-mode anion exchange HPLC column.•The method is validated for analyzing aflatoxin in M1 milk-based samples.•The method is successfully adapted to patulin in apple-based samples.

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关键词

Aflatoxin M1,Patulin,Food analysis,Mixed-mode cation exchange SPE,Mixed-mode anion exchange HPLC

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