Silver tungstate microcrystals and their performance over several clinical multidrug resistant microorganisms
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS(2022)
摘要
In this paper, we report the screening antimicrobial properties against several pathogenic microorganisms of silver tungstate microcrystals synthesized by the hydrothermal method at 120 degrees C for 12 h. These microcrystals were structurally characterized using the X-ray diffraction (XRD) and Rietveld refinement, where the ortho-rhombic structure (alpha-Ag2WO4) with space group and point group of Pn2n and C-2v(10), respectively. In according, the Raman spectrum and infrared spectrum are characteristic of pure alpha phase of silver tungstate exhibiting the main characteristic bands of orthorhombic structure. Thorough UV-vis by diffuse reflectance employing the Tauc's method the obtained optical band gap (E-gap) was 3.02(3) eV. While, the survey spectrum and high resolution Ag3d, O1s and W4f by X-ray photoelectron spectroscopy (XPS) are shown all biding energy peaks of characteristic elements of silver tungstate as well as, confirming the presence of Ag-0 for silver nanoparticles. Several rod-like microcrystals were archived by field emission scanning electron microscopy (FE-SEM), all these, exhibiting high definition and grown of silver nanoparticles with the increase of exposure time by electrons gun. Finally, the screening antimicrobial properties of alpha-Ag2WO4 confirm the high antimicrobial activity for main gram-positive and gram-positive bacteria with minimum inhibitory concentration (MIC) less than positive control (TIENAM). Therefore, the alpha-Ag2WO4 microcrystals synthesized have been exhibited promissory prop-erties in biomedical applications, particularly, in the multi-drugs gram-positive and gram-negative stains control.
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关键词
alpha-Ag2WO4, Screening, Antimicrobial, Synthesis
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