Two structural types of dithiocarbamato-chlorido complexes of mercury(II): Preparation, supramolecular self-assembly, solid-state 13C and 15N NMR characterisation and thermal behaviour of pseudo-polymeric compounds of [Hg2(S2CNBu2)2Cl2] and [Hg4(S2CNiBu2)6][Hg2Cl6]

Olga Loseva,Tatyana A. Rodina,Faiz Ullah Shah,Anton Smolentsev,Oleg N. Antzutkin,Alexander Ivanov

Inorganica Chimica Acta（2022）

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摘要

•Binuclear heteroleptic dibutyldithiocarbamato-chlorido complex of mercury(II)•Double ionic mercury(II) complex including diisobutyldithiocarbamato/chlorido ligands.•13C, 15N MAS NMR characteristics of dithiocarbamate ligands bound to mercury(II)•Pseudo-polymeric chains involving intermolecular/interionic secondary interactions.•Thermal behavior of dithiocarbamato-chlorido-mercury(II) complexes.

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关键词

Heteroleptic dithiocarbamato-chlorido mercury(II) complexes,Pseudo-polymer compounds,Supramolecular self-assembly,Secondary (Hg…S, Hg…Cl) interactions,Solid-state heteronuclear (13C, 15N) CP-MAS NMR spectroscopy,Thermal transformation of substances

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