MicroED characterization of a robust cationic σ-alkane complex stabilized by the [B(3,5-(SF₅)₂C₆H₃)₄]⁻ anion, via on-grid solid/gas single-crystal to single-crystal reactivity

Laurence R. Doyle,Emily A. Thompson,Arron L. Burnage,Adrian C. Whitwood,Huw T. Jenkins,Stuart A. Macgregor,Andrew S. Weller

Dalton Transactions（2022）

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摘要

The thermally and chemically robust σ-alkane complex [Rh(Cy2PCH2CH2PCy2)(norborane)][B(3,5-(SF5)2C6H3)4] is characterized by micro-electron diffraction using on-grid single-crystal to single-crystal reactivity.

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MicroED characterization of a robust cationic σ-alkane complex stabilized by the [B(3,5-(SF5)2C6H3)4]− anion, via on-grid solid/gas single-crystal to single-crystal reactivity

MicroED characterization of a robust cationic σ-alkane complex stabilized by the [B(3,5-(SF₅)₂C₆H₃)₄]⁻ anion, via on-grid solid/gas single-crystal to single-crystal reactivity