Enone-promoted decarboxylation of trans-4-hydroxy-l-proline in flow: a side-by-side comparison to batch

Rowan L. Pilkington,Madeleine A. Dallaston,G. Paul Savage,Craig M. Williams,Anastasios Polyzos

Reaction Chemistry & Engineering（2021）

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摘要

An efficient and scalable enone-promoted method for the decarboxylation of trans-4-hydroxy-proline has been developed in flow to provide access to (R)-pyrrolidin-3-ol hydrochloride using biomass-derived isophorone.

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