An Improved Synthesis of Bromotetrazole
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE（2022）
摘要
A new efficient synthesis of 5-bromotetrazole is presented. The free acid bromotetrazole was synthesized in a straightforward reaction analogous to the production of nitrotetrazole. Its sodium salt was readily produced via acid/base salt metathesis. Both products were characterized chemically and as energetic materials by H-1 and C-13 NMR, IR, High Resolution Mass Spectrometry, x-ray crystallography, TGA, impact and friction tests.
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关键词
Energetic materials, Tetrazoles, Improved synthesis, Heterocycles
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