Supporting Information Supramolecular Superparamagnetic Nanocomposites based on Magnetite Filled Unentangled Terpyridine Functionalized Polymer

semanticscholar(2020)

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摘要
Materials. All chemicals were purchased from Sigma-Aldrich (Merck) or Acros. Solvents of analytical grade were used unless otherwise stated. n-Butylacrylate was passed through a short column filled with activated basic aluminum oxide (Brockmann Grade I) before use. Anhydrous Dimethylsulfoxide (DMSO) from Sigma-Aldrich was used as received. 2,2Azobis(isobutyronitrile) (AIBN) was recrystallized from diethyl ether. Thin layer chromatography (TLC) were made on TLC aluminum oxide 60 F254 neutral plates from Merck. Column chromatography was performed using neutral aluminum oxide (Brockmann Grade I, 50–200 mm).
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