Iron Catalyzed Beta-C(Sp(2))-H Alkylation Of Enamides

Sylvain Bertho,Radhouan Maazaoui,Damla Torun,Ismael Dondasse,Raoudha Abderrahim,Cyril Nicolas,Isabelle Gillaizeau

NEW JOURNAL OF CHEMISTRY（2021）

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摘要

An attractive and cheap alternative approach was developed for the beta-C(sp(2))-H (fluoro)alkylation of a range of cyclic and acyclic non-aromatic enamides using either FeCl2 as a catalyst or a stoichiometric amount of nontoxic iron powder. This reaction is regioselective and exhibits broad substrate scope and good functional group tolerance.

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