Gas Ion Source Performance Of The Environmicadas At Hekal Laboratory, Debrecen, Hungary

RADIOCARBON(2021)

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摘要
A coupled accelerator mass spectrometer-gas interface system has been successfully operating at the Hertelendi Laboratory of Environmental Studies, Debrecen, Hungary, since 2013. Over the last 6 years more than 500 gas targets were measured below 100 mu g carbon content for carbon isotopic composition. The system was tested with blanks, OxII, IAEA-C1, IAEA-C2, and IAEA-C7 standards. The performance of our instrumentation shows good agreement with other published gas-interface system data and also shows a quite good agreement with the nominal value of international standard samples. There is a measurable but quite small memory effect after modern samples, but this does not significantly affect the final results. Typical ion currents at the low energy side were between 10-15 mu A with a 5% CO2 in He mixing ratio. The relative errors average +/- 6% for samples greater than or equal to 10 mu gC sample with mean count rates of 300 counts per microgram C for OxII. The blank is comparable with other systems, which is 0.0050 +/- 0.0018 (FC)-C-14 or 34,000-47,000 yr BP, which allows for the routine measurement of both of small environmental and archeological samples.
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关键词
AMS, gas interface system, gas ion source, MICADAS, radiocarbon
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