Highly Versatile Gum Acacia Based Swellable Microgels Encapsulating Cobalt Nanoparticles; An Approach to Rapid and Recoverable Environmental Nano-catalysis
JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS(2021)
摘要
Lyophilic microgels based on Gum Acacia (GAC) were synthesized at room temperature and normal pressure. Briefly, high yield of the spherical shaped microgels of size ≤ 50 µm was obtained via introducing linear GAC and divinyl sulfone (DS) in the reverse micelle cores of NBSS in the stirring gasoline. The GAC microgels were then utilized as synthetic micro-templates for fabricating their nanocomposites with Cobalt (Co), to subsequently produce GAC-Co nanocomposite microgels. The as synthesis GAC based microgels and the GAC-Co microgels were characterized through FTIR, TGA, DSC, SEM, EDS, and TEM. Different amounts of GAC-Co microgels were used as nano-catalyst for the degradation of poisonous aromatic compounds and an Azo dye in aqueous medium. Briefly, 1 g GAC-Co microgels degraded 100 mL (250 ppm solution) of each the aforementioned compounds in ≤ 25 min at neutral pH. The increase in the kinetic parameter i.e., rate constant (k app ) value with increase in the GAC-Co nanocomposite microgels amounts manifests the positive impact of the fabricated nano-catalyst on these compounds degradation at room temperature.
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关键词
Nanocomposite microgels, In situ, Nanocatalyst, Aromatic, Methyl orang
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