MICROSCOPIC AND ELECTROCHEMICAL CHARACTERIZATION OF ALUMINA CERAMIC FILMS DEVELOPED ONTO 316L STAINLESS STEEL BY MICRO-ARC OXIDATION IN PLASMA ELECTROLYSIS

Elisabeta Coaca, Oana Alice Rusu,Alexandru Horia Marin, Lucian Velciu,Maria Mihalache, Victor Aurel Andrei,Teodor Visan

UNIVERSITY POLITEHNICA OF BUCHAREST SCIENTIFIC BULLETIN SERIES B-CHEMISTRY AND MATERIALS SCIENCE(2018)

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摘要
The objective of this paper was to prepare and characterize alumina coatings developed on AISI 316L stainless steel by aluminizing treatment using micro-arc plasma oxidation in an aqueous solution containing 0.1 M NaAlO2 and 0.05 M NaOH. The obtained films were characterized by SEM microscopy and EDS analysis as well as by Tafel polarization curves and electrochemical impedance spectroscopy. Comparative results for steel samples subjected previously to two different surface pre-treatments (oxidation either by cyclic voltammetry in 0.1 M NaOH or in an autoclave with deionised water) were discussed.
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关键词
aluminium oxide films,micro-arc oxidation in plasma electrolysis,AISI 316L stainless steel,SEM microscopy,potentiodynamic polarization curves,EIS spectroscopy
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