Asymmetric [N-I-N] + halonium complexes.

Jas S Ward,Giorgia Fiorini,Antonio Frontera,Kari Rissanen

CHEMICAL COMMUNICATIONS（2020）

引用 33|浏览8

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摘要

The first asymmetric halogen-bonded iodonium complexes [I(py)(4-DMAP)]PF6(2c) and [I(py)(4-Etpy)]PF6(2e) were preparedvia[N-Ag-N](+)-> [N-I-N](+)cation exchange of their analogous 2-coordinate silver complexes. The complexes were characterised by(1)H and(1)H-N-15 HMBC NMR spectroscopy, and single crystal X-ray crystallography.

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