Direct fluorination of poly-2,6-dimethyl-1,4-phenylene oxide in perfluorinated liquid medium

Ilya A. Blinov,Dmitrii A. Mukhortov,Yurii P. Yampolskii,Nikolay A. Belov,Alexander Yu. Alentiev,Sergey V. Chirkov,Galina N. Bondarenko, Yulia V. Kostina,Sergey A. Legkov, Alexander M. Perepuchov,Marina P. Kambur,Pavel S. Kambur,Valentin V. Kapustin,Olesia N. Vozniuk, Ekaterina S. Kurapova

Journal of Fluorine Chemistry（2020）

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摘要

•Powder of poly-2,6-dimethyl-1,4-phenylene oxide was fluorinated using gaseous fluorine in the liquid perfluorinated medium.•Two different types of fluorinated polymers were obtained.•The fluorinated polymers were tested by DSC and ATR-FTIR, 13C, 19F NMR spectroscopy and their structure was ascertain.

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关键词

poly-2,6-dimethyl-1,4-phenylene oxide,direct fluorination,gas-liquid reactor,perfluorodecalin,perfluorinated polymer

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