TCDuino: Development of an Inexpensive Microcontroller-Based Thermal Conductivity Detector for Quantification of Gas Mixtures

Bradley A. Owen,Nicholas C. Starvaggi, Taylor I. Mensah, Isaac N. Mills

JOURNAL OF CHEMICAL EDUCATION(2020)

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摘要
Thermal conductivity is generally the tool of choice for quantification of fixed gases, particularly lighter-than-air gases. Unfortunately, gas chromatography-thermal conductivity detectors (GC-TCDs) are difficult to introduce in first- and second-year chemistry courses where the cost and number of instruments, as well as the space required, is impractical. In this article, the authors describe the development of a small, inexpensive microcontroller-based TCD for undergraduate teaching and research laboratory experiments which utilizes a matched pellistor pair to quantify hydrogen. The total cost of materials is under $200, including the microcontroller, electronics, TCD pellistor pair, and the mechanical parts which serve as the housing and analysis chamber.
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关键词
First-Year Undergraduate,Second-Year Undergraduate,Undergraduate Research,Computer-Based Learning,Laboratory Instruction,Laboratory Equipment/Apparatus,Laboratory Computing/Interfacing,Instrumental Methods,Analytical Chemistry,Gases
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