Validation of an ultra-sensitive detection method for steroid esters in plasma for doping analysis using positive chemical ionization GC-MS/MS.

Pieter Van Renterghem, Wouter Viaene,Wim Van Gansbeke, Juliana Barrabin,Michele Iannone,Michael Polet,Guy T'Sjoen,Koen Deventer,Peter Van Eenoo

Journal of Chromatography B（2020）

引用 19|浏览11

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摘要

•Ultra-sensitive GC-MS/MS detection method for testosterone and nandrolone esters.•Designed and validated for easy implementation in doping control laboratories.•Limit of detection between 10 and 200 pg/ml.•Detection of long acting testosterone undecanoate preparation to 86 days.

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关键词

Steroid esters,Direct detection,Testosterone,Doping control,GC-MS/MS,Chemical ionisation

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