Synthesis of porous organic cage CC3 via solvent modulated evaporation

Jolie M. Lucero,Jacek B. Jasinski,Miao Song,Dongsheng Li,Lili Liu,Jun Liu,James J. De Yoreo,Praveen K. Thallapally,Moises A. Carreon

Inorganica Chimica Acta（2020）

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摘要

•A novel synthetic method for the formation of porous organic cage CC3 is demonstrated.•CC3 was synthesized via Modulating Solvent Evaporation.•MSER relies on the gradual evaporation of dichloromethane from a diluted concentration of CC3 precursors.•The slow solvent evaporation modulated by relative humidity allowed enough time for the formation of CC3.

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关键词

Porous organic cages,Modulated evaporation,Crystal growth

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