A Novel Copper-Catalyzed Synthesis Of N-Monosubstituted 2-Alkynimi-Damides From 1-Alkynes And Trichloroacetamidines

Hossein Fasihi Dastjerdi,Manijeh Nematpour,Elham Rezaee,Mehdi Jahani,Sayyed Abbas Tabatabai

LETTERS IN ORGANIC CHEMISTRY（2020）

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摘要

A one-pot Cu-catalyzed synthesis of functionalized alkynyl imidamide by terminal alkynes, trichloroacetonitrile and aniline or benzyl amine is reported. The compounds were produced via coupling reaction of terminal alkynes with trichloroacetamidine. This method was performed under mild, ligand-free conditions and easy work-up method.

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关键词

Terminal alkynes,copper iodide,alkynylimidamide,cross-coupling,aniline,one-pot reaction

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