Synthesis and biological evaluation of calcioic acid.

Olivia B Yu,Tania R Mutchie,Elliot S Di Milo,Leggy A Arnold

Steroids（2020）

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摘要

•Accomplished the first total synthesis of calcioic acid.•Calcioic acid binds to the vitamin D receptor.•Calcioic acid does not activate the vitamin D receptor mediated transcription of CYP24A1.

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关键词

25OHD3,CYP24A1,1,25(OH)2D3,VDR,TLC,DCM,EtOAc,NMR,CHCl3,TBSOTf,18-crown-6,DIBAL-H,TBME,MeOH,t-BuOH,TFA,PDC,NH4Cl,n-BuLi,THF,TBAF,PIPES,NP-40,LBD,DMSO,HEPES,CMV

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