Catalytic Cycloaminomethylation of Aminobenzamides with 1,3-Bis[dimethylamino(methoxy)methyl]thiourea

R. R. Khairullina,T. V. Tyumkina,A. R. Geniyatova,M. F. Abdullin,A. G. Ibragimov

Russian Journal of General Chemistry（2019）

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摘要

Efficient methods of the synthesis of cyclophanes containing the thiourea moiety via the reaction of o-, m- , and p -aminobenzamides with 1,3-bis(dimethylaminomethyl)thiourea or 1,3-bis(methoxymethyl)thiourea using NiCl 2 ·6H 2 O and SmCl 3 ·6H 2 O as catalysts have been developed.

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关键词

cycloaminomethylation, aminobenzamides, bis(N,N-dimethylamino)methane, thiourea, cyclophanes

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