Expanding production regions of α-form and β-form glycine using an antisolvent crystallization method assisted by N2 fine bubbles

Masakazu Matsumoto,Yoshinari Wada, Shota Maesawa,Toshihiko Hiaki,Kaoru Onoe

Advanced Powder Technology（2019）

引用 7|浏览9

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摘要

•Fine bubbles enable α and β-form glycine production at lower bulk supersaturation.•Glycine polymorphs change via local supersaturation at fine gas–liquid interfaces.•A carbon number decrease in alcohol enhances local supersaturation around fine bubbles.•Polymorphs are controllable by carbon number and generation rate of supersaturation.

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关键词

Fine bubbles,Gas–liquid interface,Antisolvent crystallization,Unstable form,Metastable form

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