Synthesis and characterization of poly([Eu or Dy] 1,1’-ferrocenediyl-bis(H-phosphinates))

R. P. Shekurov,L. H. Gilmanova,M. N. Khrizanforov,S. O. Strekalova,Y. H. Budnikova,T. P. Gerasimova,S. A. Katsyuba,V. A. Miluykov

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS（2019）

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摘要

Metal-organic frameworks [M2L3](n) have been synthesized using ferrocene-based ligand bearing phosphinic groups L=1,1'-ferrocenediyl-bis(H-phosphinic acid)) and M(III) = Eu, Dy. Structures of complexes 1 and 2 are studied by IR and powder XRD analyses and shown to be isomorphic. The thermal decomposition of the synthesized compounds was studied by differential scanning calorimetry and thermogravimetry. [GRAPHICS] .

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Lanthanides,phosphinate,rare-earth metal,ferrocene derivative

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