Analysis of sulfonamides, tilmicosin and avermectins residues in typical animal matrices with multi-plug filtration cleanup by liquid chromatography–tandem mass spectrometry detection

Journal of Chromatography B(2017)

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摘要
•A veterinary drugs multi-residue method in animal samples was developed.•Modified QuEChERS and ultrasound-assisted extraction were optimized.•M-PFC method with n-Hexane delipidation were used for cleanup.•Solvents, ultrasonic process, sorbents, m-PFC procedure were optimized.
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关键词
Veterinary drugs,Residues analysis,Animal matrices,Multi-plug filtration cleanup
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