Synthesis and structures of a palladium macrocycle, a six-membered palladacycle, and a palladium compartment complexes: [Pd(L1)Cl], [Pd(NH2CH2CH2CH2NH2)Cl2], and [Pd(L2)] (HL1 = (E)-2-)(((3-aminopropyl)imino)methyl)-6-methoxyphenol; H2L2 = N,N′-bis(3-methoxysalicylidenimino-1,3-diaminopropane)

Polyhedron（2016）

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摘要

The palladium compartment complex [Pd(L2)] (H2L2=N,N′-bis(3-methoxysalicylidenimino-1,3-diaminopropane)) was prepared from the free bis(imine) ligand (H2L2) and [Pd(PhCN)2Cl2] or Pd(OAc)2 in methanol.

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关键词

Palladium compartment complex,Schiff-base ligand,Crystal structures,Thermal conversion,Cyclohexane-like palladacycle

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