General Method for Selective Mono-Boc Protection of Diamines and Thereof

Felipe A. Servín,José A. Romero,Gerardo Aguirre,Douglas B. Grotjahn,Ratnasamy Somanathan,Daniel Chávez

JOURNAL OF THE MEXICAN CHEMICAL SOCIETY（2017）

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摘要

Here we report a simple and efficient protocol for selectively diamine protection with Boc using Me3SiCl or SOCl2 as HCl source in "one-pot" procedure. This methodology is extended to 1,2- to 1,8-diamines to obtain the corresponding mono-Boc protected diamines.

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关键词

Chiral,cyclohexane-1,2-diamine,1,2-diphenylethane-1,2-diamine,Boc monoprotection,diamines

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