Anodic Synthesis of New Benzofuran Derivatives Using Active Methylene Group at Platinum Electrode

Russian Journal of Electrochemistry(2018)

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摘要
A facile and Eco-compatible synthesis of benzofuran derivatives ( 4a–4h ) has been carried out at platinum electrode by electrochemical oxidation of catechol in the presence of active methylene groups. Electro- organic synthesis has been performed in an undivided cell at ambient conditions. The products of electrolysis have been purified and characterized by FTIR, 1 H NMR and 13 C NMR and mechanism was deduced by voltammetric studies.
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关键词
anodic oxidation,catechol,Michael addition,controlled potential electrolysis (CPE),cyclic voltammetry
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