Electrochemical Formation of 3,5-Diimido-1,2-dithiolanes by Dehydrogenative Coupling

Valentina M Breising,Tile Gieshoff, Anton Kehl,Vincent Kilian,Dieter Schollmeyer,Siegfried R Waldvogel

Organic Letters（2018）

引用 19|浏览6

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摘要

A synthetic approach to the cyclic disulfide moiety of 3,5-diimido-1,2-dithiolane derivatives starting with readily available precursors including the electrochemical coupling of dithioanilides is developed. The electrochemical key step provides sustainable synthetic access in high yields, using a very simple electrolysis setup.

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