Surface-Enhanced Raman Spectroscopic Analysis Of N-6-Benzylaminopurine Residue Quantity In Sprouts With Gold Nanoparticles

JOURNAL OF ENVIRONMENTAL SCIENCE AND HEALTH PART B-PESTICIDES FOOD CONTAMINANTS AND AGRICULTURAL WASTES(2018)

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摘要
A rapid and quantitative method for the determination of N-6-Benzylademine (N-6-BA) was established through the application of surface-enhanced Raman spectroscopy (SERS). The Raman peak intensities of N-6-BA at 1002cm(-1) positively correlated to N-6-BA concentrations in sprout extracts. The R-2 reached 0.99, and RSDs calculated below 10% at the concentration range of 0.1 approximate to 5g mL(-1). The average recoveries were 80.0% approximate to 98.2% for blank samples intentionally contaminated at differing levels of 0.04, 0.4, and 1g g(-1). The whole procedure, including sample preparation and SERS detection, did not exceed 30min for a set of 6 samples. This study indicates that SERS is a promising technique for rapid tracing analysis and on-site testing of N-6-BA.
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关键词
N-6-Benzylademine,surface-enhanced Raman spectroscopy,rapid detection,quantitative analysis,label free detection
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